Conformations and Energetics of B- and Y-Ions in Peptoid Fragmentation

Lead Author Major

Pre-Pharmacy

Lead Author Status

Senior

Format

Poster Presentation

Faculty Mentor Name

Jianhua Ren

Faculty Mentor Department

Chemistry

Graduate Student Mentor Name

Yuntao Zhang

Graduate Student Mentor Department

Chemistry

Abstract/Artist Statement

Peptoids, peptide-mimicking polymers, are man-made molecules that are not susceptible to protease degradation. It has shown high potential in pharmaceutics, such as artificial pulmonary surfactants and Alzheimer’s treatment. Unfortunately, the broadening of applications has been hindered by the lack of optimal ways to efficiently sequence peptoids. To gain knowledge about their fragmentation pathways and help develop peptoid sequencing methods, a series of model peptoids have been designed, and their fragmentation patterns have been investigated thoroughly. The energetics and structures of the N-terminal fragments, B-ions, and C-terminal fragments, Y-ions, were also examined to rationalize experimental observations.

A series of peptoids varying in length were designed. The initial conformations of B-ions, Y-ions, and their “neutral” pairs were generated based on “chemistry intuition.” Conformer search using MMFF method was completed, and sequential optimizations were executed. With the energetics and conformations, the computational outputs were used to examine the differences between channels to form each observed ion.

Y-ions were generally found in higher abundance compared to B-ions, and the energy differences between the Y- and B-ion channels (E(Y) – E(B)) at each amide position were calculated. For positions where different sizes of Y- and B-ions are formed, the larger ion tends to be energetically favored. As the amide bond cleavage moves from C-terminus to N-terminus, the Y-ion channel becomes more favored. In longer Y-ions, more hydrogen bonding interactions allow for adequate stabilization of the charged cation, while oxazolone ring stabilization has less importance for longer B-ions. Based on this research endeavor, we have found that peptoid fragmentation patterns can be correlated to the energetics of peptoid fragmentation using computational chemistry.

Location

Virtual

Start Date

25-4-2020 1:00 PM

End Date

25-4-2020 3:00 PM

This document is currently not available here.

Share

COinS
 
Apr 25th, 1:00 PM Apr 25th, 3:00 PM

Conformations and Energetics of B- and Y-Ions in Peptoid Fragmentation

Virtual

Peptoids, peptide-mimicking polymers, are man-made molecules that are not susceptible to protease degradation. It has shown high potential in pharmaceutics, such as artificial pulmonary surfactants and Alzheimer’s treatment. Unfortunately, the broadening of applications has been hindered by the lack of optimal ways to efficiently sequence peptoids. To gain knowledge about their fragmentation pathways and help develop peptoid sequencing methods, a series of model peptoids have been designed, and their fragmentation patterns have been investigated thoroughly. The energetics and structures of the N-terminal fragments, B-ions, and C-terminal fragments, Y-ions, were also examined to rationalize experimental observations.

A series of peptoids varying in length were designed. The initial conformations of B-ions, Y-ions, and their “neutral” pairs were generated based on “chemistry intuition.” Conformer search using MMFF method was completed, and sequential optimizations were executed. With the energetics and conformations, the computational outputs were used to examine the differences between channels to form each observed ion.

Y-ions were generally found in higher abundance compared to B-ions, and the energy differences between the Y- and B-ion channels (E(Y) – E(B)) at each amide position were calculated. For positions where different sizes of Y- and B-ions are formed, the larger ion tends to be energetically favored. As the amide bond cleavage moves from C-terminus to N-terminus, the Y-ion channel becomes more favored. In longer Y-ions, more hydrogen bonding interactions allow for adequate stabilization of the charged cation, while oxazolone ring stabilization has less importance for longer B-ions. Based on this research endeavor, we have found that peptoid fragmentation patterns can be correlated to the energetics of peptoid fragmentation using computational chemistry.